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ASTM E595-93(2003)e2

Historical Revision

Standard Test Method for Total Mass Loss and Collected Volatile Condensable Materials from Outgassing in a Vacuum Environment

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1.1 This test method covers a screening technique to determine volatile content of materials when exposed to a vacuum environment. Two parameters are measured: total mass loss (TML) and collected volatile condensable materials (CVCM). An additional parameter, the amount of water vapor regained (WVR), can also be obtained after completion of exposures and measurements required for TML and CVCM.

1.2 This test method describes the test apparatus and related operating procedures for evaluating the mass loss of materials being subjected to 125°C at less than 7 X 10-3 Pa (5 X 10 -5 torr) for 24 h. The overall mass loss can be classified into noncondensables and condensables. The latter are characterized herein as being capable of condensing on a collector at a temperature of 25°C.

Note 1—Unless otherwise noted, the tolerance on 25 and 125°C is ± 1°C and on 23°C is ± 2°C. The tolerance on relative humidity is ± 5%.

1.3 Many types of organic, polymeric, and inorganic materials can be tested. These include polymer potting compounds, foams, elastomers, films, tapes, insulations, shrink tubings, adhesives, coatings, fabrics, tie cords, and lubricants. The materials may be tested in the "as-received" condition or prepared for test by various curing specifications.

1.4 This test method is primarily a screening technique for materials and is not necessarily valid for computing actual contamination on a system or component because of differences in configuration, temperatures, and material processing.

1.5 The criteria used for the acceptance and rejection of materials shall be determined by the user and based upon specific component and system requirements. Historically, TML of 1.00% and CVCM of 0.10% have been used as screening levels for rejection of spacecraft materials.

1.6 The use of materials that are deemed acceptable in accordance with this test method does not ensure that the system or component will remain uncontaminated. Therefore, subsequent functional, developmental, and qualification tests should be used, as necessary, to ensure that the material's performance is satisfactory.

1.7 This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


SDO ASTM: ASTM International
Document Number E595
Publication Date Oct. 1, 2003
Language en - English
Page Count 8
Revision Level 93(2003)e2
Supercedes
Committee E21.05
Publish Date Document Id Type View
May 1, 2015 E0595-15 Revision
Dec. 1, 2007 E0595-07 Revision
Nov. 1, 2006 E0595-06 Revision
Oct. 1, 2003 E0595-93R03E02 Revision
April 1, 2021 E0595-15R21 Reaffirmation
Oct. 1, 2003 E0595-93R03E01 Reaffirmation
April 10, 1999 E0595-93R99 Reaffirmation