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ASTM E352-93(2000)e1

Historical Revision

Standard Test Methods for Chemical Analysis of Tool Steels and Other Similar Medium- and High-Alloy Steels

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1.1 These test methods cover the chemical analysis of tool steels and other similar medium- and high-alloy steels having chemical compositions within the following limits:

Element Concentration Range, %
Aluminum0.005 to 1.5
Boron 0.001 to 0.10
Carbon 0.03 to 2.50
Chromium0.10 to 14.0
Cobalt 0.10 to 14.0
Copper 0.01 to 2.0
Lead 0.001 to 0.01
Manganese0.10 to 15.00
Molybdenum0.01 to 10.00
Nickel 0.02 to 4.00
Nitrogen0.001 to 0.20
Phosphorus0.002 to 0.05
Silicon 0.10 to 2.50
Sulfur 0.002 to 0.40
Tungsten0.01 to 21.00
Vanadium0.02 to 5.50

1.2 The test methods in this standard are contained in the sections indicated below:

Sections
Carbon, Total, by the Combustion-ThermalConductivity Method2a
Carbon, Total, by the Combustion GravimetricalMethod (0.05 to 2.50 %) 78
Chromium by the Atomic Absorption Method(0.006 to 1.00 %)174
Chromium by the Peroxydisulfate Oxidation-Titration Method(0.10 to 14.00 %)184
Chromium by the Peroxydisulfate-OxidationTitrimetric Method2 b
Cobalt by the Ion-Exchange-PotentiometricTitration Method (2 to 14 %)52
Cobalt by the Nitroso-R-Salt PhotometricMethod(0.10 to 5.0 %)60
Copper by the Neocuproine Photometric Method (0.01 to 2.00 %) 89
Copper by the Sulfide Precipitation-Electrodeposition Gravimetric Method (0.01 to 2.0 %)70
Lead by the Ion-Exchange-Atomic AbsorptionMethod (0.001 to 0.001 %)99
Nickel by the Dimethylglyoxime GravimetricMethod(0.1 to 4.0 %)144
Manganese by the Periodate PhotometricMethod(0.10 to 5.00 %)8
Molybdenum by the Ion Exchange-8-Hydro-xyquinoline Gravimetric Method 203
Molybdenum by the Photometric Method(0.01 to 1.50 %)162
Phosphorus by the Alkalimetric Method(0.01 to 0.05 %)136
Phosphorus by the Molybdenum Blue Photo-metric Method (0.002 to 0.05 %)18
Silicon by the Gravimetric Method(0.10 to 2.50 %)45
Sulfur by the Gravimetric Method 2c
Sulfur by the Combustion-Iodate TitrationMethod(0.005 to 0.4 %)36
Sulfur by the Chromatographic GravimetricMethod 2b
Tin by the Solvent Extraction-Atomic Absorp-tion Method (0.002 to 0.10 %)152
Vanadium by the Atomic Absorption Method(0.006 to 0.15 %)193

1.3 Test methods for the determination of several elements not included in this standard can be found in Test Methods E30 and Test Methods E1019.

1.4 Some of the concentration ranges given in 1.1 are too broad to be covered by a single test method and therefore this standard contains multiple test methods for some elements. The user must select the proper test method by matching the information given in the Scope and Interference sections of each test method with the composition of the alloy to be analyzed.

1.5 The values stated in SI units are to be regarded as standard. In some cases, exceptions allowed in Practice E380 are also used.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards statements are given in Section 5 and in special "Warning" paragraphs throughout these test methods.


SDO ASTM: ASTM International
Document Number E352
Publication Date Jan. 1, 2000
Language en - English
Page Count 29
Revision Level 93(2000)e1
Supercedes
Committee E01.01
Publish Date Document Id Type View
Nov. 15, 2023 E0352-23 Revision
July 1, 2018 E0352-18E01 Revision
July 1, 2018 E0352-18 Revision
Feb. 1, 2013 E0352-13 Revision
Jan. 1, 2000 E0352-93R00E01 Revision
June 1, 2006 E0352-93R06 Reaffirmation