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ASTM E1413-07

Historical Revision

Standard Practice for Separation of Ignitable Liquid Residues from Fire Debris Samples by Dynamic Headspace Concentration onto an Adsorbent Tube

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1.1 This practice describes the procedure for separation of small quantities of ignitable liquid residues from fire debris samples using the absorption/elution method of headspace concentration.

1.2 Both positive and negative pressure systems are described.

1.3 While this practice is suitable for successfully extracting ignitable liquid residues over the entire range of concentration, the headspace concentration methods are best used when a high level of sensitivity is required due to a very low concentration of ignitable liquid residues in the sample.

1.4 Alternate separation and concentration procedures are listed in Section 2.

This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.


This practice is useful for preparing extracts from fire debris for later analysis by gas chromatography, GC/MS, or GC/IR.

This is a very sensitive separation procedure, capable of isolating quantities smaller than 0.1 μL of ignitable liquid residue from a sample.

4.2.1 Actual recovery will vary, depending on several factors, including adsorption temperature, container size, and competition from the sample matrix.

This is a potentially destructive technique. Portions of the sample subjected to this procedure may not be suitable for re-sampling. Therefore, a portion of the sample extract should be saved for potential future analysis. Consider using passive headspace concentration as described in Practice E 1412.

SDO ASTM: ASTM International
Document Number E1413
Publication Date April 15, 2007
Language en - English
Page Count 3
Revision Level 07
Supercedes
Committee E30.01
Publish Date Document Id Type View
June 1, 2019 E1413-19 Revision
Aug. 15, 2013 E1413-13 Revision
April 15, 2007 E1413-07 Revision
June 1, 2006 E1413-06 Revision
Nov. 10, 2000 E1413-00 Revision
May 1, 2005 E1413-00R05 Reaffirmation