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ASTM D800-05

Historical Revision

Standard Test Methods of Chemical Analysis of Industrial Metal Cleaning Compositions (Withdrawn 2023)

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1.1 These test methods describe the procedures for the chemical analysis of industrial metal cleaning compositions in solid, paste, or liquid form. These cleaning compositions may contain caustic alkalies, silicates, phosphates, chromates, carbonates, bicarbonates, borates, sulfates, sulfites, nitrates, chlorides, soaps, rosin, sulfonated wetting agents, anti-foaming agents, organic bases, organic solvents, organic coupling agents, and sometimes inorganic acid salts or organic acids. Occasionally, such cleaning compositions may contain sulfonated oils; in such cases, reference should be made to Method D 500. The examination under a low power microscope or magnifying glass, supplemented by a few qualitative tests, will often indicate the number of components and their identity.

1.2 The analytical methods appear in the following order:

Section
Preparation of Sample4
Total Alkalinity as Na2O5-8
Total Fatty Acids (and Rosin)9 and 10
Na2O Combined with Fatty Acids (and Rosin)11 and 12
Anhydrous Soap13
-Rosin (McNicoll Test Method):
Qualitative14 and 15
Quantitative16-19
Total Silica Calculated as SiO220-23
Phosphates:
Qualitative24 and 25
Quantitative26-18
Combined Sodium and Potassium Oxides34-37
Chlorides38-40
Sulfates41-43
Water, Distillation Test Method44-47
Carbon Dioxide by Evolution-Absorption Test Method48-52
Loss at 105C53 and 54
Total Matter Insoluble in Alcohol55-57
Free Alkali58-60
Synthetic Detergent or Wetting Agent61 and 62
Volatile Hydrocarbons63-67
Loss on Ignition68 and 69
Report70 and 71

1.3This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Material Safety Data Sheets are available for reagents and materials. Review them for hazards prior to usage. See for a specific hazards statement.


These test methods describe the procedures for the chemical analysis of industrial metal cleaning compositions in solid, paste, or liquid form. These cleaning compositions may contain caustic alkalies, silicates, phosphates, chromates, carbonates, bicarbonates, borates, sulfates, sulfites, nitrates, chlorides, soaps, rosin, sulfonated wetting agents, anti-foaming agents, organic bases, organic solvents, organic coupling agents, and sometimes inorganic acid salts or organic acids. Percentage of total sodium oxide, percentage of potassium oxide, percentage of free sodium hydroxide, percentage of water, percentage of losses, percentage of matter insoluble in alcohol, percentage of fatty acids, percentage of rosin, percentage of synthetic detergent or wetting agent, percentage of silica, percentage of phosphorus pentoxide, percentage of carbon dioxide, percentage of sodium chloride, percentage of sodium sulfate, and percentage of volatile hydrocarbons test methods shall be performed to conform with the specified requirements.


SDO ASTM: ASTM International
Document Number D800
Publication Date May 1, 2005
Language en - English
Page Count 12
Revision Level 05
Supercedes
Committee D12.12
Publish Date Document Id Type View
Jan. 1, 2014 D0800-05R14 Revision
May 1, 2005 D0800-05 Revision
March 10, 1997 D0800-91R97 Revision