Logo

ASTM D5827-09e1

Historical Revision

Standard Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography

$83.00

$83.00

$149.40

$0.00

$0.00

$0.00



Sub Total (1 Item(s))

$ 0.00

Estimated Shipping

$ 0.00

Total (Pre-Tax)

$ 0.00


Stay effortlessly up-to-date with the latest standard revisions. When new versions are released, they're automatically charged and delivered to you, ensuring seamless compliance.

...

1.1 This test method covers the chemical analysis of engine coolant for chloride ion by high-performance ion chromatography (HPIC). Several other common anions found in engine coolant can be determined in one chromatographic analysis by this test method.

1.2 This test method is applicable to both new and used engine coolant.

1.3 Coelution of other ions may cause interferences for any of the listed anions. In the case of unfamiliar formulations, identification verification should be performed by either or both fortification and dilution of the sample matrix with the anions of interest.

1.4 Analysis can be performed directly by this test method without pretreatment, other than dilution, as required by the linear ranges of the equipment. Table 1 indicates several applicable anions and approximate detection limits.

1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to its use.

TABLE 1 Analytes and Minimum Detection Limits

AnalyteDetection Limit, mg/LA
Chloride (Cl) 2.0
Nitrite (NO2) 5.0
Bromide (Br) 4.0
Nitrate (NO3) 7.1
o-Phosphate (HPO4)220.0
Sulfate (SO4)2 8.0
Oxalate (C2O4)212.0

A Determined using 100-μL sample volume. Sample diluted 99 + 1 (v/v) with chromatographic eluant 30-μS/cm full scale, suppressed conductivity detection. Dionex AS4ASC column with AG4ASC guard columns. Other systems will require MDL determinations using chosen dilution factors, eluants, columns, and detector.


This test method provides for the qualitative and quantitative determination of common anions in engine coolant in the milligrams per litre to low percent range and requires only a few millilitres or microlitres of sample per test, with results available in less than 30 min. Acceptable levels of chloride and other anions vary with manufacturer's blending specifications and applicable ASTM minimum or maximum specifications.

SDO ASTM: ASTM International
Document Number D5827
Publication Date March 1, 2009
Language en - English
Page Count 6
Revision Level 09e1
Supercedes
Committee D15.04
Publish Date Document Id Type View
June 1, 2022 D5827-22 Revision
March 1, 2009 D5827-09E01 Revision
March 1, 2009 D5827-09 Revision
Jan. 1, 1995 D5827-95 Revision
May 1, 2015 D5827-09R15 Reaffirmation
Sept. 10, 1995 D5827-95R02 Reaffirmation