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ASTM D4768-11

Current Revision

Standard Test Method for Analysis of 2,6-Ditertiary-Butyl Para-Cresol and 2,6-Ditertiary- Butyl Phenol in Insulating Liquids by Gas Chromatography

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1.1 This test method covers the determination by gas chromatography of 2,6-ditertiary-butyl para-cresol and 2,6-ditertiary-butyl phenol in new and used insulating liquids at concentrations up to 0.5 %. It includes the determination in Type I and II insulating mineral oils as specified in Specification D3487, but has also been used to measure these inhibitors in other insulating liquids, such as esters and high fire-point hydrocarbons.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

In new electrical insulating oil, this test method provides a quantitative measure of the amounts of 2,6-ditertiary-butyl para-cresol and 2,6-ditertiary-butyl phenol that have been added to the oil. In a used oil, the test measures the amount of these inhibitors remaining in the oil. This test method is suitable for manufacturing control, specification acceptance, and service evaluation.

This test method is used to separate, identify, and quantify the inhibitors with minimal interference and matrix effects.

This test method has also been used successfully to determine the inhibitor concentrations in other insulating liquids such as esters and high-temperature hydrocarbons.

SDO ASTM: ASTM International
Document Number D4768
Publication Date Aug. 1, 2011
Language en - English
Page Count 3
Revision Level 11
Supercedes
Committee D27.03
Publish Date Document Id Type View
Aug. 1, 2011 D4768-11 Revision
March 10, 2003 D4768-03 Revision
Jan. 1, 1996 D4768-96 Revision
Dec. 1, 2019 D4768-11R19 Reaffirmation