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ASTM C1287-03

Historical Revision

Standard Test Method for Determination of Impurities in Uranium Dioxide by Inductively Coupled Plasma Mass Spectrometry

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1.1 This test method covers the determination of 67 elements in uranium dioxide samples and nuclear grade uranium compounds and solutions without matrix separation by inductively coupled plasma mass spectrometry (ICP-MS). The elements are listed in Table 1. These elements can also be determined in uranyl nitrate hexahydrate (UNH), uranium hexafluoride (UF6), triuranium octoxide (U3O8) and uranium trioxide (UO 3) if these compounds are treated and converted to the same uranium concentration solution.

1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.For a specific warning statement, see Note 1.

Note 1—Warning: The ICP-MS is a source of intense ultra-violet radiation from the radio frequency induced plasma. Protection from radio frequency radiation and UV radiation is provided by the instrument under normal operation.

1.3 The elements boron, sodium, silicon, phosphorus, potassium, calcium and iron can be determined using different techniques. The analyst's instrumentation will determine which procedure is chosen for the analysis.

1.4 The test method for technetium-99 is given in Annex A1.


SDO ASTM: ASTM International
Document Number C1287
Publication Date July 10, 2003
Language en - English
Page Count 9
Revision Level 03
Supercedes
Committee C26.05
Publish Date Document Id Type View
Jan. 1, 2018 C1287-18 Revision
June 1, 2010 C1287-10 Revision
July 10, 2003 C1287-03 Revision
Sept. 10, 1995 C1287-95 Revision
Sept. 10, 1995 C1287-95R01 Reaffirmation