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ASTM C1206-02(2010)

Current Revision

Standard Test Method for Plutonium by Iron (II)/Chromium (VI) Amperometric Titration

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1.1 This test method covers the determination of plutonium in unirradiated nuclear-grade plutonium dioxide, uranium-plutonium mixed oxides with uranium (U)/plutonium (Pu) ratios up to 21, plutonium metal, and plutonium nitrate solutions. Optimum quantities of plutonium to measure are 7 to 15 mg.

1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.

1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

All plutonium materials covered in this test method are used in the preparation of nuclear-reactor fuels. In order to be suitable for this purpose, the materials must meet specified criteria for plutonium content. This test method is used to verify the plutonium content.

A primary standard dichromate such as that available from National Institute of Standards and Technology (NIST) or a dichromate traceable to a primary standard such as New Brunswick Laboratory (NBL) plutonium standard, is required for this technique.

SDO ASTM: ASTM International
Document Number C1206
Publication Date Jan. 1, 2010
Language en - English
Page Count 5
Revision Level 02(2010)
Supercedes
Committee C26.05
Publish Date Document Id Type View
Jan. 1, 2010 C1206-02R10 Revision
Jan. 10, 2002 C1206-02 Revision
Jan. 10, 2002 C1206-91R96 Reaffirmation